Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 4117-09-3, name is 7-Bromo-1-heptene, A new synthetic method of this compound is introduced below., Recommanded Product: 7-Bromo-1-heptene
Take N-(1-adamantane)-3-indolecarboxamide (322 mg, 1.10 mmol)In dimethylformamide (5ml),Sodium hydride (88 mg, 2.20 mmol) was slowly added under ice-water bath.After the absence of bubbles, 7-bromo-1-heptene (244 mg, 1.30 mmol) was added.After 30 min reaction, the intermediate (7-(3-((1-adamantamine) formyl))-indolyl)heptene (187 mg, 44%) was obtained.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; East China Normal University; Shanghai Bangyao Biological Technology Co., Ltd.; Zhang Hankun; Pang Xiufeng; Liu Mingyao; Jiang Beier; Liu Zhitao; Yu Weiwei; Liang Qiuwen; (41 pag.)CN109879790; (2019); A;,
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