Electric Literature of 58971-11-2, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 58971-11-2, name is 3-Bromophenethylamine belongs to bromides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Add 200 mL of dichloromethane to the three-neck bottle.32.0 g of 3-bromophenethylamine and 17.0 g of triethylamine at 10 C,16.0 g of methyl chloroformate was added dropwise, and after completion of the dropwise addition, the reaction was continued for 2 hours.Add 300 mL of hot water, separate the organic phase, and wash with ammonium chloride solution.Wash with saturated brine and dry over anhydrous sodium sulfate.Concentration gave 38.4 g (96.7%) of methyl 3-bromophenethylcarbamate.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 3-Bromophenethylamine, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Nantong University; Zhu Jinli; Ding Jinjin; Wang Miao; Zhu Xiting; Tian Dan; Sun Tongming; Tian Liang; Zhu Liangliang; Hong Chuanxia; (5 pag.)CN103880745; (2018); B;,
Bromide – Wikipedia,
bromide – Wiktionary