Related Products of 1647-26-3, The chemical industry reduces the impact on the environment during synthesis 1647-26-3, name is 1-Bromo-2-cyclohexylethane, I believe this compound will play a more active role in future production and life.
General procedure: A mixture of 3-methyl-hypoxanthine (0.59 mmol, 89 mg) and anhydrous potassium carbonate (amounts, see Tables in the article) in dry DMSO (23 mL) was stirred under N2 at ambient temperature for 1 h. Alkyl halide (amounts, see Tables in the article) in dry DMSO (5 mL) was added over 5 min by a syringe pump (rate 60 mL/h). The reaction mixture was stirred for at ambient temperature for the time given in the article. The mixture was filtered, the filtrate concentrated in vacuo and the residue was purified by flash chromatography on SiO2. In cases where the product was not completely pure after chromatography, the material isolated was cooled to 5 C in a 50 mL round bottom flask, and stirred moderately for 2 h in distilled hexane (50 mL). The solid was allowed to settle (1 h) and most of the hexane was removed carefully by a pipette, leaving a small volume, so as not to remove the fine particles of product at the bottom. The remaining hexane was removed by concentration in vacuo.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1-Bromo-2-cyclohexylethane, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Chamgordani, Elahe Jafari; Paulsen, Jan; Gundersen, Lise-Lotte; Tetrahedron Letters; vol. 57; 44; (2016); p. 4926 – 4929;,
Bromide – Wikipedia,
bromide – Wiktionary