In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 67567-26-4, name is 4-Bromo-2,6-difluoroaniline belongs to bromides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. SDS of cas: 67567-26-4
4-Bromo-2,6-difluoroaniline (65A, 0.50Og, 2.4mmol) was combined with sodium methanesul finale (0.98g, 9.6mmol), cuprous triflate benzene complex (0.121g, 0.24mmol), and N,N’-dimethylethylencdiamine (0.027mL, 0.23mmol) in DMF (5mL). The mixture was heated to 150 C and allowed to stir at this temperature for 24 hours, then was concentrated in vacuo and purified using PLC to provide compound 65B as a yellow solid.
The synthetic route of 67567-26-4 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; SCHERING CORPORATION; WO2009/55331; (2009); A2;,
Bromide – Wikipedia,
bromide – Wiktionary