Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 52997-43-0, name is 7-(Bromomethyl)pentadecane, This compound has unique chemical properties. The synthetic route is as follows., SDS of cas: 52997-43-0
250 mL of a condenser equipped with a magnetic stirrer and a reflux condenserAdd three bottles4-bromothiophenol10 g (52.89 mmol),N, N-dimethylformamide100 mL,Anhydrous potassium carbonate 10.94 g (79.33 mmol)Argon protection,Stirred at room temperature for 30 minutes,With a constant pressure dropping funnel1-bromo-2-hexyl decane16.2 mL (52.89 mmol) was added dropwise to the reaction system and the reaction was gradually progressedThe temperature was raised to 85 C and the reaction was carried out for 24 hours. The reaction was completed, cooled to room temperature, the reaction solution was poured into 150 mL of ice water,Stirring for 10 minutes, and then petroleum ether as extractant extraction 3 times, each 100mL, the organic phase, organic phase with distilled waterWash 3 times, each time 150mL. The organic phase was dried over anhydrous sodium sulfate, filtered, and the filtrate was spin-dried using a rotary evaporator to giveThe crude product was obtained by column chromatography using petroleum ether as eluent4-bromo-1- (2-hexylDecylthio) benzene(Colorless transparent liquid, 20.12 g, yield 92.0%)
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 52997-43-0.
Reference:
Patent; Xiangtan University; Zhao, Bin; Liu, Hailu; Huang, Meihua; Tang, Bo; (8 pag.)CN106380431; (2017); A;,
Bromide – Wikipedia,
bromide – Wiktionary